CHEM2711 - Spectroscopic Experiments - Medical Science Assignment Help

Assignment Task

Please download this quiz and answer all questions as clearly and completely as possible. Submit an electronic version of your solutions on FLO. You are required to work on this quiz on your own. You may not work with other students or discuss this quiz with other students. You are allowed to ask the Topic Coordinator questions during the Quiz period in case any question is not clear.

1. Outline two spectroscopic experiments that could be used to distinguish the azide starting material and the amine product in the following reaction. Be explicit on the type of experiment and how your spectrum will be interpreted.

2. The C-H stretch for CHCl3 appears at 3034 cm-1 in its IR spectrum. The C-D stretch for CDCl3 appears at 2230 cm-1. What accounts for this difference?

3. An unknown compound with the molecular formula C3H5N has the following IR, 1H NMR, and 13C spectra. Propose a structure for the compound. Assign diagnostic peaks in the IR spectrum and fully assign the NMR spectra. Label your assignments directly on the spectra provided.

4. Explain how NMR can be useful in determining stereochemistry of a molecule. Support your answer with reference to a specific molecule or molecules and discuss the specific signals and analysis required to determine the stereochemical assignment.

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